UNIVERSITAS AIRLANGGA



Detail Article

Berkala Ilmiah Kimia Farmasi

ISSN 2302-8270

Vol. 2 / No. 1 / Published : 2013-06

Order : 2, and page :9 - 15

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Original Article :

Validasi metode kromatografi gas-spektrometri massa untuk penetapan kadar residu endosulfan dalam kubis

Author :

  1. Dini Tri Anggraini*1
  2. Riesta Primaharinastiti*2
  3. Isnaeni*3
  1. Mahasiswa Fakultas Farmasi
  2. Dosen Fakultas Farmasi
  3. Dosen Fakultas Farmasi

Abstract :

The purpose of this study is to develop and validate a simple method suitable for   analysis of trace amounts of endosulfan in cabbage. Cabbage samples were extracted with acetone and endosulfan was partitioned into dichloromethane/n-hexane (1:1, v/v). Final determination was performed by gas chromatography with mass spectrometry. Recovery studies were performed at 0.02 mg/kg fortification level of each compound (endosulfan I, endosulfan II, endosulfan sulfat) and the recoveries obtained ranged 69.67% to 124.02% with coefficient of variation values of 5.56-11.54%. The method showed good linearity over the range assayed 2-6 µg/mL and the detection and quantification limits for endosulfan studied varied, 0.1273 µg/mL to 0.1469 µg/mL and 0.856 µg/mL to 0.4451 µg/mL respectively.    

Keyword :

GC-MS, , endosulfan, pesticides, validation, cabbage,


References :

Bempah, C.K., Buah-Kwofie, A., Enimil, E., and Blewu, B. ,(2011) Residues of organochlorine pesticides in vegetables marketed in Greater Accra region of Ghana Journal : Food Control, (25)





Archive Article

Cover Media Content

Volume : 2 / No. : 1 / Pub. : 2013-06
  1. Validasi Spektrofotometri Visible Untuk Penentuan Kadar Formalin Dalam Daging Ayam
  2. Validasi Metode Kromatografi Gas-spektrometri Massa Untuk Penetapan Kadar Residu Endosulfan Dalam Kubis
  3. Sintesis Dan Uji Aktivitas Antikanker Senyawa 1-(2-klorobenzoiloksi)urea Dan 1-(4-klorobenzoiloksi)urea
  4. Pengaruh Gugus Metoksi Posisi Orto (o) Dan Para (p) Pada Benzaldehida Terhadap Sintesis Turunan Khalkon Dengan Metode Kondensasi Aldol
  5. Modifikasi Struktur N-fenilurea Menjadi Senyawa Baru N-benzoilfenilurea Dan 4-fluorobenzoilfenilurea Serta Uji Aktivitasnya Sebagai Penekan Susunan Saraf Pusat
  6. Aktivitas Antinociceptiv Dan Uji In Silico Terhadap Cyclooxygenase Dari Asam P-metoksisinamat Dan Asam M-metoksisinamat
  7. Docking Dan Modifikasi Struktur Senyawa Baru Turunan Parasetamol

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