UNIVERSITAS AIRLANGGA



Detail Article

Berkala Ilmiah Kimia Farmasi

ISSN 2302-8270

Vol. 2 / No. 2 / Published : 2013-11

Order : 3, and page :13 - 19

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Original Article :

Penetapan kadar formalin dalam ayam potong yang diambil di pasar tradisional surabaya timur

Author :

  1. Sudjarwo*1
  2. Asri Darmawati*2
  3. Vivi Wahyu Hariyanti*3
  1. Dosen Fakultas Farmasi
  2. Dosen Fakultas Farmasi
  3. Mahasiswa Fakultas Farmasi

Abstract :

Formalin is not permitted for food preservative because it is toxic for human. The aim of this study was to determine the illicit additive of formalin in chicken meat which were taken from East Surabaya traditional markets. The number of samples were 100 slices of chicken meat which were taken from 15 markets in East Surabaya. Samples were collected from Pucang Anom, Manyar, Tambak Rejo, Pacar Keling, Gubeng Masjid, Indrakila, Sutorejo, Bratang, Kendangsari, Gebang, Keputih, Tenggilis, Pahing, Soponyono, and Rungkut traditional markets. Formalin in samples were detected by chromotropic acid in concentrated sulfuric acid as reagent, prior to determine quantitatively. Intensity of the violet-red color obtained was determined with spectrophotometry at the wavelength of 567.5 nm. Validation of this method showed that detection limit was 0.134 ppm and quantitation limit was 0.446 ppm. Linearity was obtained in the range of (0.395 to 1.581) ppm, coefficient correlation (r) of 0.9967 with regression line of y = 0.216x + 0.023. Recovery of formaldehyde in samples were (73.26 ± 8.01)% with KV of 10.93 %. This study obtained that formalin was not detected in all of the samples.    

Keyword :

Formalin, chicken meat, chromotropic acid, Vis-Spectrophotometry, East Surabaya Traditional Markets,


References :

Carr, G.P. and Wahlich, J.C., ,(1990) A practical approach to method validation in pharmaceutical and analysis Journal : Journal of Pharmaceutical Biomedical Analysis

Fagnani, E., Melios, C.B., Pezza L., and Pezza H.R.,,(2003) Chromotropic acid-formaldehyde reaction in strongly acidic media. The role of dissolved oxygen and replacement of concentrated sulfuric acid Journal : Talanta, Vol. 60





Archive Article

Cover Media Content

Volume : 2 / No. : 2 / Pub. : 2013-11
  1. Uji Aktivitas Analgesik Senyawa Baru Turunan Parasetamol Pada Mencit (mus Musculus) Dengan Metode Hot Plate
  2. Validasi Metode Kromatografi Lapis Tipis-densitometri Untuk Penetapan Kadar Kolkisin Dalam Infus Daun Kembang Sungsang (gloriosa Superba Linn.)
  3. Penetapan Kadar Formalin Dalam Ayam Potong Yang Diambil Di Pasar Tradisional Surabaya Timur
  4. Pemodelan Molekul Dan Hubungan Kuantitatif Struktur-aktivitas Sitotoksik Turunan Benzoilurea Sebagai Antitumor
  5. Kandungan Salisilat Bebas Dalam Tablet Asetosal Yang Beredar Di Surabaya
  6. Pemanfaatan Daun Trembesi (samanea Saman) Dalam Mengadsorpsi Logam Berat Timbal
  7. Perbandingan Aktivitas Penekan Susunan Saraf Pusat Senyawa Baru N-benzoilfenilurea Dan 4-nitrobenzoilfenilurea