UNIVERSITAS AIRLANGGA



Detail Article

Berkala Ilmiah Kimia Farmasi

ISSN 2302-8270

Vol. 4 / No. 1 / Published : 2015-06

Order : 3, and page :12 - 20

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Original Article :

Validasi metode ekstraksi quechers untuk analisis multiresidu pestisida pada wortel secara kromatografi gas-spektrometri massa

Author :

  1. Riesta Primaharinastiti*1
  2. Setyo Prihatiningtyas*2
  3. Mochamad Yuwono*3
  1. Dosen Fakultas Farmasi
  2. Dosen Fakultas Farmasi
  3. Dosen Fakultas Farmasi

Abstract :

The purpose of this study is to develop a simple method for organochlorine and orfanophosphate residues determination in carrot. Residues are separated from carrot samples using QuEChERS kit for extraction method. Determination of the pesticides was performed by gas chromatography with mass spectrometry detector. Recovery studies were performed at 0.02 mg/kg fortification level of each compound and the recoveries obtained ranged 66.29 to 111.60% with coefficient of variation values of 2.12-20.88 %. The method showed good linearity over the range assayed 0.7-7.0 µg/mL and the detection and quantification limits for organochlorine studied varied, 0.21-0.24 µg/mL to 0.612-0.74 µg/mL. This method showed satisfactory extraction efficiencies combined with simplicity of use and low solvent consumption. Therefore this method is suitable for routine analysis of triadimefon in cabbage

Keyword :

GC-MS, organochlorine, organophosphate, pesticides, carrot,


References :

Horwitz, William, ,(2000) Official Methods of Analysis of AOAC International Marryland : Gaithersburg,





Archive Article

Cover Media Content

Volume : 4 / No. : 1 / Pub. : 2015-06
  1. Pengaruh Pasta Tomat (lycopersicon Esculentum Mill.) Pada Daya Hambat Lactobacillus Acidophilus Fncc-0051 Dan Lactobacillus Plantarum Fncc-0027 Terhadap Candida Albicans
  2. Sintesis N’-benzilidenbenzohidrazida Dan N’-(4-metoksibenziliden)-benzohidrazida Dengan Material Awal Metilbenzoat
  3. Validasi Metode Ekstraksi Quechers Untuk Analisis Multiresidu Pestisida Pada Wortel Secara Kromatografi Gas-spektrometri Massa
  4. Profil Bioautogram Bakteriosin Dalam Sediaan Susu Probiotik
  5. Aktifitas Antimikroba Fraksi-fraksi Dari Ekstrak Etil Asetat Jamur Endofit Yang Diisolasi Dari Aglaia Odorata Lour.
  6. Modifikasi Struktur Dan Prediksi Aktivitas Antikanker Senyawa Baru Turunan Aliltiourea Secara In Silico
  7. Penapisan Aktivitas Antioksidan Kombinasi Yogurt Dan Jus Tomat Dibandingkan Vitamin C